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| Analytical
Services |
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The Sophisticated Analytical
Instrument Facility has several highly sophisticated
and modern analytical equipment. Analytical
services are offered to both internal and
external users. The facilities are availed
by about 250 internal users and 500 external
users annually. More than 80% of the external
users comprise researchers from universities
and colleges. Researchers from national
laboratories and industries constitute the
rest. Some of the major facilities being
provided are:
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Mass spectrometry |
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NMR spectrometry |
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Electron microscopy.
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Routine facilities such
as IR/UV, GLC |
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| Service to the outside users
is provided on payment basis. The samples
required for test also vary have to be sent
as per the requirement of the analysis. |
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| Charges
for the Analytical Services and the requirement
of test Sample |
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Service Charges
*
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S.No.
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Facility |
Requirements
on test sample |
Charges in
Rs. / hr. / sample/spectrum |
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1.
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Mass Spectrometers
Joel SX-102(EI/CI/FAB)
MicromassQuarter2
(APCI,ESI,LCMS,MS/MS
Shimadzu QP -2000
(GC/MS)
Micromass TofSpec2e
MALDI TOF MS
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1-2 mg
Nature of the sample, meting point,solibility,elements
present, expected m.wt & structure,
GC conditions and GC trace for GC/MS,
LC condition & LC trace for LCMS.Compound
should be metal free and volatile
below
250 0C for EI/CI
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1200/-
per hr .or part thereof with a minimum
of Rs 1200/- per sample for additional
facilities such as GCMS,CI,FAB, MIKES,
APCI,ESI, LC/MS & MS/MS, MALDI TOF
MS |
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NMR
Spectrometers
Bruker DRX-300
(300MHz FT NMR
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2-4mg
Nature of compound, eg, carcinogenic,
radio active, solubility, lachrymatory,
explosive hygroscopic etc structural
formula (contemplated known).
Required amount of sample
Must be soluble in 0.5-1.0ml
Of deuteratd solvent. |
600/-
per hr.with minimum of Rs.600/-per sample
for 1D spectrum (1H, 13C
& other nuclei)
1200/-
per hr .or part there of with a minimum
of Rs 1200/-per spectrum for 2D spectroscopy
and inverseexperiments.
100/- Extra charges for deuterated solvents
Other than CDCL3 and D2O. |
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FTIR
Spectropotometers
Shimadzu 8201PC
(4000\-350 cm-1)
Perkin Elmer
Spectrum RxI
(4000-450 cm-1) |
5-10
mg
Kbr /Njuol/CsI/CHCL3,
Nature (hygroscopic ,explosive etc.)
-do-
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450/-
per spectrum or Rs 600/- per hr when
extending time averaging is required
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UV/VS
Spectrophotometer
Perkin Elmer Hitachi 320 lambda 15 |
5-10
mg
spectrum range (200-850nm), nature and
solvent qualitative /quantitative |
240/-
per sample
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Gas
liquid
Chromotograph
Varian vista 6000 |
2-5
mg
Nature of compound ,
Solubility, melting point /
Boiling point ,column (if known )
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300
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per hr. per sample |
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Elemental
analyzers
Heraeus Vario EL III Carlo Erba 1108
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10
mg
other elements present,
approximate % of nitrogen
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300/-
per element per sample
(CHNS&O) |
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Polar
meter
Rudolf Autopol III
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20
mg
sample should be completely
soluble in the suggested solvent &free
from foreign particles
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300/-
per sample |
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Electron
Microscopes
TEM
FEI-Philips Tecnai 12
SEM
FEI-Philips XL-30 |
User
should get confirmation
Before sending samplexs
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Rs.
1000/-per sample
Rs.3000/- for TEM sample preparation
including sectioning.
Rs.1000/-pre sample.
Rs. 1200/-for SEM sample preparation
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* Charges
given are Private Industries
National Laboratries and Private Government
Small Scale Industries will pay 3/5th of these
charges;
Educational Institutions will pay 1/5 th of
the charges. |
| Note
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The analytical data /
spectra are provided only for research
/ development purposes. These can not
be used as certificates in legal disputes.
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Service charges are payable
in advance by crossed bank in favor
of the
Director, Central Drug Research Institute,
Lucknow-226001. |
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Samples and payment should
be sent preferably in the same cover.
Separate Sample should be sent for deferent
analysis .Samples are not analysed till
Payment is received |
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Maximum 3samples for Mass
2samples for 13c,19f,31pNMRand 10 samples
For other types of analysis are accepted
at a time. |
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Please send the samples
is quantity as mentioned in the brochure
.Samples are Not recovered .unless a
special request is made. |
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In all correspondence
related to analysis our referenced must
be mentioned |
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Radio -active material
should be clearly mentioned and handed
over personally. |
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Unstable and axplosive
compounds are not accepted for analysis. |
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Services are
rendered to only those users who regularly
give us feed -back about the and use
of the result ,e.g., thesis,patent,
process publication etc. |
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Research fellows and students
are advised to send there application
and samples through their Supervisor
or Head of department. |
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Interpretation of spectra
is not undertaken normally . In special
cases this service can be provided on
payment on extra charges . |
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All
Communication should be addressed to
Head
Sophisticated analytical Instrument Facility,
Central Drug Research Institute,
Post Box No.173,
Lucknow 226001 |
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website
copyright © Central Drug Research Institute.
All rights reserved.
No part of this should be Downloaded or used
in any way other than the non-commercial purposes
without prior permission of the Director,
CDRI. |
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